8. NMR Chemical Shift Calculations

NMR spectroscopy is one of the most important analytical tools for solution phase chemistry. The significance of NMR spectroscopy is based on its ability to distinguish a particular nucleus with respect to its molecular environment. Key parameters obtained from experimental spectra are the chemical shifts of NMR active nuclei as well as their coupling parameters with the respective neighbours. In the following we will focus on the theoretical calculation of isotropic shielding values ​​as a measure of different chemical environments (Calculation of NMR Isotropic Shieldings) and their correspondence with experimentally measured chemical shifts (Conversion of Isotropic Shieldings to Chemical Shifts and Positional Averaging of Shielding Values). The accuracy of NMR chemical shift predictions benefits substantially from selecting appropriate (that is: specifically optimized) basis sets and chemically related reference systems.

  1. Calculation of NMR Isotropic Shieldings
  2. Conversion of Isotropic Shieldings to Chemical Shifts
  3. Positional Averaging of Shielding Values
  4. Influence of Theoretical Methods
  5. Selecting Appropriate Reference Systems